Efficient exfoliation and downsizing of Sb2S3 and Bi2S3 layered compounds by using scalable bipolar electrochemistry on their suspensions in aqueous media are here demonstrated. The resulting samples were characterized in detail by transmission electron microscopy, energy-dispersive X-ray spectroscopy, and X-ray photoelectron spectroscopy; their electrochemistry toward hydrogen evolution was also investigated. Hydrogen evolution ability of exfoliated Sb2S3 and Bi2S3 was investigated and compared to the bulk counterparts.
Bibliographical noteFunding Information:
M.P. acknowledges the financial support of Grant Agency of the Czech Republic (EXPRO: 19-26896X).
M.P. acknowledges the financial support of Grant Agency of the Czech Republic (EXPRO: 19‐26896X).
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All Science Journal Classification (ASJC) codes
- Organic Chemistry