Direct synthesis of acyl azides from carboxylic acids by the combination of trichloroacetonitrile, triphenylphosphine and sodium azide

Joong Gon Kim, Doook Jang

Research output: Contribution to journalArticle

17 Citations (Scopus)

Abstract

Various carboxylic acids were converted into acyl azides in excellent yields by treating with trichloroacetonitrile, triphenylphosphine and sodium azide at room temperature. The reaction was applicable to the preparation of dipeptide without rearrangement.

Original languageEnglish
Pages (from-to)2072-2074
Number of pages3
JournalSynlett
Issue number13
DOIs
Publication statusPublished - 2008 Aug 1

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Sodium Azide
Azides
Dipeptides
Carboxylic Acids
Temperature
trichloroacetonitrile
triphenylphosphine

All Science Journal Classification (ASJC) codes

  • Organic Chemistry

Cite this

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title = "Direct synthesis of acyl azides from carboxylic acids by the combination of trichloroacetonitrile, triphenylphosphine and sodium azide",
abstract = "Various carboxylic acids were converted into acyl azides in excellent yields by treating with trichloroacetonitrile, triphenylphosphine and sodium azide at room temperature. The reaction was applicable to the preparation of dipeptide without rearrangement.",
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Direct synthesis of acyl azides from carboxylic acids by the combination of trichloroacetonitrile, triphenylphosphine and sodium azide. / Kim, Joong Gon; Jang, Doook.

In: Synlett, No. 13, 01.08.2008, p. 2072-2074.

Research output: Contribution to journalArticle

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