Effect of reaction solvent on the hydrogenation of isophthalonitrile for meta-xylylendiamine preparation

Sung Wook Row; Tae Young Chae; Kye Sang Yoo; Sang Duek Lee; Do Weon Lee; Yonggun Shul

doi:10.1002/cjce.5450850614

Effect of reaction solvent on the hydrogenation of isophthalonitrile for meta-xylylendiamine preparation

Sung Wook Row, Tae Young Chae, Kye Sang Yoo, Sang Duek Lee, Do Weon Lee, Yonggun Shul

Department of Chemical and Biomolecular Engineering

Research output: Contribution to journal › Article › peer-review

9 Citations (Scopus)

Abstract

This study focused on the effects of reaction solvent on the hydrogenation of isophthalonitrile (IPN) to produce m-Xylylenediamine (MXDA) over Ni-based commercial catalyst. The hydrogenation was carried out using various reaction solvents such as 1-methylimidazole, mesitylene, benzyl ether and isopropanol under various reaction conditions. It was observed that 1-methylimiazole outperformed the other reaction solvent, exhibiting a high MXDA yield and producing a low concentration of undesirable products.

Original language	English
Pages (from-to)	925-928
Number of pages	4
Journal	Canadian Journal of Chemical Engineering
Volume	85
Issue number	6
DOIs	https://doi.org/10.1002/cjce.5450850614
Publication status	Published - 2007 Dec

All Science Journal Classification (ASJC) codes

Chemical Engineering(all)

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abstract = "This study focused on the effects of reaction solvent on the hydrogenation of isophthalonitrile (IPN) to produce m-Xylylenediamine (MXDA) over Ni-based commercial catalyst. The hydrogenation was carried out using various reaction solvents such as 1-methylimidazole, mesitylene, benzyl ether and isopropanol under various reaction conditions. It was observed that 1-methylimiazole outperformed the other reaction solvent, exhibiting a high MXDA yield and producing a low concentration of undesirable products.",

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AU - Row, Sung Wook

AU - Chae, Tae Young

AU - Yoo, Kye Sang

AU - Lee, Sang Duek

AU - Lee, Do Weon

AU - Shul, Yonggun

PY - 2007/12

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AB - This study focused on the effects of reaction solvent on the hydrogenation of isophthalonitrile (IPN) to produce m-Xylylenediamine (MXDA) over Ni-based commercial catalyst. The hydrogenation was carried out using various reaction solvents such as 1-methylimidazole, mesitylene, benzyl ether and isopropanol under various reaction conditions. It was observed that 1-methylimiazole outperformed the other reaction solvent, exhibiting a high MXDA yield and producing a low concentration of undesirable products.

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Effect of reaction solvent on the hydrogenation of isophthalonitrile for meta-xylylendiamine preparation

Abstract

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