Facile Synthesis of Palladium-Nanoparticle-Embedded N-Doped Carbon Fibers for Electrochemical Sensing

Kyubin Shim; Zhong Li Wang; Tasnima Haque Mou; Yoshio Bando; Abdulmohsen Ali Alshehri; Jeonghun Kim; Md Shahriar A. Hossain; Yusuke Yamauchi; Jung Ho Kim

doi:10.1002/cplu.201800139

Facile Synthesis of Palladium-Nanoparticle-Embedded N-Doped Carbon Fibers for Electrochemical Sensing

Kyubin Shim, Zhong Li Wang, Tasnima Haque Mou, Yoshio Bando, Abdulmohsen Ali Alshehri, Jeonghun Kim, Md Shahriar A. Hossain, Yusuke Yamauchi, Jung Ho Kim

Department of Chemical and Biomolecular Engineering

Research output: Contribution to journal › Article › peer-review

8 Citations (Scopus)

Abstract

In recent years, there have been many studies on metal/carbon hybrid materials for electrochemical applications. However, reducing the metal content in catalysts is still a challenge. Here, a facile synthesis of palladium (Pd) nanoparticle-embedded N-doped carbon fibers (Pd/N-C) through electropolymerization and reduction methods is demonstrated. The as-prepared Pd/N-C contains only 1.5 wt % Pd. Under optimal conditions, bisphenol A is detected by using amperometry in two dynamic ranges from 0.1 to 10 μm and from 10 to 200 μm, and the obtained correlation coefficients are close to 0.9836 and 0.9987, respectively. The detection limit (DL) for bisphenol A is determined to be 29.44 (±0.77) nm.

Original language	English
Pages (from-to)	401-406
Number of pages	6
Journal	ChemPlusChem
Volume	83
Issue number	5
DOIs	https://doi.org/10.1002/cplu.201800139
Publication status	Published - 2018 May

Bibliographical note

Funding Information:
Z.W. thanks the Japan Society for Promotion of Science (JSPS) for providing the standard postdoctoral fellowship. This study was supported by an Australian Research Council (ARC) Future Fellow (FT150100479), the Suzuken Memorial Foundation, JSPS KAKENHI (grant numbers 17H05393 and 17K19044). This study was supported by the Deanship of Scientific Research (DSR), King Abdula-ziz University, Jeddah, under grant number KEP-7-130-39.

Publisher Copyright:
© 2018 Wiley-VCH Verlag GmbH & Co. KGaA, Weinheim

All Science Journal Classification (ASJC) codes

Chemistry(all)

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10.1002/cplu.201800139

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title = "Facile Synthesis of Palladium-Nanoparticle-Embedded N-Doped Carbon Fibers for Electrochemical Sensing",

abstract = "In recent years, there have been many studies on metal/carbon hybrid materials for electrochemical applications. However, reducing the metal content in catalysts is still a challenge. Here, a facile synthesis of palladium (Pd) nanoparticle-embedded N-doped carbon fibers (Pd/N-C) through electropolymerization and reduction methods is demonstrated. The as-prepared Pd/N-C contains only 1.5 wt % Pd. Under optimal conditions, bisphenol A is detected by using amperometry in two dynamic ranges from 0.1 to 10 μm and from 10 to 200 μm, and the obtained correlation coefficients are close to 0.9836 and 0.9987, respectively. The detection limit (DL) for bisphenol A is determined to be 29.44 (±0.77) nm.",

author = "Kyubin Shim and Wang, {Zhong Li} and Mou, {Tasnima Haque} and Yoshio Bando and Alshehri, {Abdulmohsen Ali} and Jeonghun Kim and Hossain, {Md Shahriar A.} and Yusuke Yamauchi and Kim, {Jung Ho}",

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AU - Alshehri, Abdulmohsen Ali

AU - Kim, Jeonghun

AU - Hossain, Md Shahriar A.

AU - Yamauchi, Yusuke

AU - Kim, Jung Ho

N1 - Funding Information: Z.W. thanks the Japan Society for Promotion of Science (JSPS) for providing the standard postdoctoral fellowship. This study was supported by an Australian Research Council (ARC) Future Fellow (FT150100479), the Suzuken Memorial Foundation, JSPS KAKENHI (grant numbers 17H05393 and 17K19044). This study was supported by the Deanship of Scientific Research (DSR), King Abdula-ziz University, Jeddah, under grant number KEP-7-130-39. Publisher Copyright: © 2018 Wiley-VCH Verlag GmbH & Co. KGaA, Weinheim

PY - 2018/5

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Facile Synthesis of Palladium-Nanoparticle-Embedded N-Doped Carbon Fibers for Electrochemical Sensing

Abstract

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