High pressure curing of phenol resin for high quality coating of glassy carbon

Seok Gi Hong, Kwang Youn Cho, Oh Hyeon Kwon, Yong Soo Cho, Seung Jo Jang

Research output: Contribution to journalArticle

Abstract

Successful coating of high quality glassy carbon is introduced by applying high pressure during the curing process of dip-coated phenol resin on graphite. The dependence of the applied pressure on the quality of the glassy carbon layer has not been reported so far. Pressure was changed from 0 to 400 psi during curing at 200°C. After carbonized at 1100°C in inert atmosphere for the 400 psicured sample, as a promising result, a thick (∼ 3 mm) and smooth glassy carbon layer could be obtained without any breakage, and the yield of carbonization was remarkably increased. It is believed that the cross-linking of resins results in decreasing volatile contents and, thus, increasing the yield of the glassy carbon. The origin of the improvement is discussed on the basis of several analytical results including FE-SEM, FT-IT and Raman spectrum.

Original languageEnglish
Pages (from-to)141-146
Number of pages6
JournalJournal of the Korean Ceramic Society
Volume48
Issue number2
DOIs
Publication statusPublished - 2011 Mar 1

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Glassy carbon
Phenol
Phenols
Curing
Resins
Coatings
Graphite
Carbonization
Raman scattering
Scanning electron microscopy

All Science Journal Classification (ASJC) codes

  • Ceramics and Composites

Cite this

Gi Hong, Seok ; Youn Cho, Kwang ; Hyeon Kwon, Oh ; Cho, Yong Soo ; Jo Jang, Seung. / High pressure curing of phenol resin for high quality coating of glassy carbon. In: Journal of the Korean Ceramic Society. 2011 ; Vol. 48, No. 2. pp. 141-146.
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High pressure curing of phenol resin for high quality coating of glassy carbon. / Gi Hong, Seok; Youn Cho, Kwang; Hyeon Kwon, Oh; Cho, Yong Soo; Jo Jang, Seung.

In: Journal of the Korean Ceramic Society, Vol. 48, No. 2, 01.03.2011, p. 141-146.

Research output: Contribution to journalArticle

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AU - Gi Hong, Seok

AU - Youn Cho, Kwang

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AB - Successful coating of high quality glassy carbon is introduced by applying high pressure during the curing process of dip-coated phenol resin on graphite. The dependence of the applied pressure on the quality of the glassy carbon layer has not been reported so far. Pressure was changed from 0 to 400 psi during curing at 200°C. After carbonized at 1100°C in inert atmosphere for the 400 psicured sample, as a promising result, a thick (∼ 3 mm) and smooth glassy carbon layer could be obtained without any breakage, and the yield of carbonization was remarkably increased. It is believed that the cross-linking of resins results in decreasing volatile contents and, thus, increasing the yield of the glassy carbon. The origin of the improvement is discussed on the basis of several analytical results including FE-SEM, FT-IT and Raman spectrum.

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