Microstructural comparison of Zr73.5Nb9Cu7Ni1Al9.5 nanostructure-dendrite composites produced by different casting techniques

K. B. Kim, J. Das, W. Löser, M. H. Lee, D. H. Kim, S. K. Roy, J. Eckert

Research output: Contribution to journalArticle

8 Citations (Scopus)

Abstract

Zr73.5Nb9Cu7Ni1Al9.5 (numbers indicate at.%) nanostructure-dendrite composites were fabricated using three different casting techniques: suction casting, centrifugal casting and arc-melting. The microstructure of the suction casting sample consists of micrometer-scale dendrites in a nanostructured matrix. However, some areas in the matrix contain nano-scale crystals together with an amorphous phase revealing an inhomogeneity of the specimen. On the contrary, the microstructures of the centrifugally-cast and the arc-melted samples are overall homogeneous, consisting of micrometer-scale dendrites that are homogeneously distributed in a nanostructured matrix. The dendrites correspond to a body centered cubic (bcc) β-Zr phase, whereas the nanostructured matrix consists of body centered tetragonal (bct) Zr2Cu-type and hexagonal close-packed (hcp) MgZn2-type phases. The comparison of the microstructures of these two alloys reveals that the formation of nano-scale twins and a disordered ω-phase in the β-Zr dendrites only happens in the centrifugally-cast sample. The differences in the phases and the microstructures between the differently prepared samples significantly influence the corresponding mechanical properties of the specimens.

Original languageEnglish
Pages (from-to)747-751
Number of pages5
JournalMaterials Science and Engineering A
Volume449-451
DOIs
Publication statusPublished - 2007 Mar 25

All Science Journal Classification (ASJC) codes

  • Materials Science(all)
  • Condensed Matter Physics
  • Mechanics of Materials
  • Mechanical Engineering

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