Abstract
Modified ZnO NPs were synthesized through a sol-gel route with an aromatic capping agent to provide a highly efficient catalyst, NS-5, for the one-pot multicomponent synthesis of various pyrimidine derivatives using a solvent-free ball milling technique. Greenness of the present method was evaluated by calculating an Ecoscale score and E-factor. Characteristics of the method include use of a recyclable catalyst, scale-up to a multigram scale, and ease of product isolation.
| Original language | English |
|---|---|
| Pages (from-to) | 1468-1475 |
| Number of pages | 8 |
| Journal | ACS Sustainable Chemistry and Engineering |
| Volume | 5 |
| Issue number | 2 |
| DOIs | |
| Publication status | Published - 2017 Feb 6 |
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All Science Journal Classification (ASJC) codes
- Chemistry(all)
- Environmental Chemistry
- Chemical Engineering(all)
- Renewable Energy, Sustainability and the Environment
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"Solvent-less" mechanochemical approach to the synthesis of pyrimidine derivatives. / Raj, Tilak; Sharma, Hemant; Mayank; Singh, Ajnesh; Aree, Thammarat; Kaur, Navneet; Singh, Narinder; Jang, Doook.
In: ACS Sustainable Chemistry and Engineering, Vol. 5, No. 2, 06.02.2017, p. 1468-1475.Research output: Contribution to journal › Article
TY - JOUR
T1 - "Solvent-less" mechanochemical approach to the synthesis of pyrimidine derivatives
AU - Raj, Tilak
AU - Sharma, Hemant
AU - Mayank,
AU - Singh, Ajnesh
AU - Aree, Thammarat
AU - Kaur, Navneet
AU - Singh, Narinder
AU - Jang, Doook
PY - 2017/2/6
Y1 - 2017/2/6
N2 - Modified ZnO NPs were synthesized through a sol-gel route with an aromatic capping agent to provide a highly efficient catalyst, NS-5, for the one-pot multicomponent synthesis of various pyrimidine derivatives using a solvent-free ball milling technique. Greenness of the present method was evaluated by calculating an Ecoscale score and E-factor. Characteristics of the method include use of a recyclable catalyst, scale-up to a multigram scale, and ease of product isolation.
AB - Modified ZnO NPs were synthesized through a sol-gel route with an aromatic capping agent to provide a highly efficient catalyst, NS-5, for the one-pot multicomponent synthesis of various pyrimidine derivatives using a solvent-free ball milling technique. Greenness of the present method was evaluated by calculating an Ecoscale score and E-factor. Characteristics of the method include use of a recyclable catalyst, scale-up to a multigram scale, and ease of product isolation.
UR - http://www.scopus.com/inward/record.url?scp=85011883202&partnerID=8YFLogxK
UR - http://www.scopus.com/inward/citedby.url?scp=85011883202&partnerID=8YFLogxK
U2 - 10.1021/acssuschemeng.6b02030
DO - 10.1021/acssuschemeng.6b02030
M3 - Article
AN - SCOPUS:85011883202
VL - 5
SP - 1468
EP - 1475
JO - ACS Sustainable Chemistry and Engineering
JF - ACS Sustainable Chemistry and Engineering
SN - 2168-0485
IS - 2
ER -