Sputtered PdO decorated TiO2 sensing layer for a hydrogen gas sensor

Jeong Hoon Lee, Seungmin Kwak, Jin Hyung Lee, Inho Kim, Yong Kyoung Yoo, Tae Hoon Lee, Young Seok Shim, Jinseok Kim, Kyu Hyoung Lee

Research output: Contribution to journalArticle

3 Citations (Scopus)

Abstract

We report a sputtered PdO decorated TiO2 sensing layer by radiofrequency (RF) sputtering methods and demonstrated gas sensing performance for H2 gas. We prepared sputtered anatase TiO2 sensing films with 200 nm thickness and deposited a Pd layer on top of the TiO2 films with a thickness ranging from 3 nm to 13 nm. Using an in situ TiO2/Pd multilayer annealing process at 550°C for 1 hour, we observed that Pd turns into PdO by Auger electron spectroscopy (AES) depth profile and confirmed decorated PdO on TiO2 sensing layer from scanning electron microscope (SEM) and atomic-force microscope (AFM). We also observed a positive sensing signal for 3, 4.5, and 6.5 nm PdO decorated TiO2 sensor while we observed negative output signal for a 13.5 nm PdO decorated one. Using a microheater platform, we acquired fast response time as 11 sec and sensitivity as 6 μV/ppm for 3 nm PdO under 33 mW power.

Original languageEnglish
Article number8678519
JournalJournal of Nanomaterials
Volume2018
DOIs
Publication statusPublished - 2018 Jan 1

Fingerprint

Chemical sensors
Hydrogen
Gases
Auger electron spectroscopy
Titanium dioxide
Sputtering
Multilayers
Microscopes
Electron microscopes
Annealing
Scanning
Sensors
titanium dioxide

All Science Journal Classification (ASJC) codes

  • Materials Science(all)

Cite this

Lee, Jeong Hoon ; Kwak, Seungmin ; Lee, Jin Hyung ; Kim, Inho ; Yoo, Yong Kyoung ; Lee, Tae Hoon ; Shim, Young Seok ; Kim, Jinseok ; Lee, Kyu Hyoung. / Sputtered PdO decorated TiO2 sensing layer for a hydrogen gas sensor. In: Journal of Nanomaterials. 2018 ; Vol. 2018.
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abstract = "We report a sputtered PdO decorated TiO2 sensing layer by radiofrequency (RF) sputtering methods and demonstrated gas sensing performance for H2 gas. We prepared sputtered anatase TiO2 sensing films with 200 nm thickness and deposited a Pd layer on top of the TiO2 films with a thickness ranging from 3 nm to 13 nm. Using an in situ TiO2/Pd multilayer annealing process at 550°C for 1 hour, we observed that Pd turns into PdO by Auger electron spectroscopy (AES) depth profile and confirmed decorated PdO on TiO2 sensing layer from scanning electron microscope (SEM) and atomic-force microscope (AFM). We also observed a positive sensing signal for 3, 4.5, and 6.5 nm PdO decorated TiO2 sensor while we observed negative output signal for a 13.5 nm PdO decorated one. Using a microheater platform, we acquired fast response time as 11 sec and sensitivity as 6 μV/ppm for 3 nm PdO under 33 mW power.",
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Lee, JH, Kwak, S, Lee, JH, Kim, I, Yoo, YK, Lee, TH, Shim, YS, Kim, J & Lee, KH 2018, 'Sputtered PdO decorated TiO2 sensing layer for a hydrogen gas sensor', Journal of Nanomaterials, vol. 2018, 8678519. https://doi.org/10.1155/2018/8678519

Sputtered PdO decorated TiO2 sensing layer for a hydrogen gas sensor. / Lee, Jeong Hoon; Kwak, Seungmin; Lee, Jin Hyung; Kim, Inho; Yoo, Yong Kyoung; Lee, Tae Hoon; Shim, Young Seok; Kim, Jinseok; Lee, Kyu Hyoung.

In: Journal of Nanomaterials, Vol. 2018, 8678519, 01.01.2018.

Research output: Contribution to journalArticle

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AU - Lee, Jeong Hoon

AU - Kwak, Seungmin

AU - Lee, Jin Hyung

AU - Kim, Inho

AU - Yoo, Yong Kyoung

AU - Lee, Tae Hoon

AU - Shim, Young Seok

AU - Kim, Jinseok

AU - Lee, Kyu Hyoung

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