Synthesis of Zirconia Colloids from Aqueous Salt Solutions

Kangtaek Lee, Arun Sathyagal, Peter W. Carr, Alon V. McCormick

Research output: Contribution to journalArticle

19 Citations (Scopus)

Abstract

We monitor the synthesis of ZrO2 colloids from dissolved ZrOCl2·8H2O using quasi-elastic light scattering and cryotransmission electron microscopy (cryo-TEM). We investigate the effects of both precursor salt concentration and pH on the final size distribution. We find that the initial pH plays the most important role in the final particle size and yield. These trends and cryo-TEM observations help elucidate the roles of nucleation, aggregation, and recrystallization.

Original languageEnglish
Pages (from-to)338-342
Number of pages5
JournalJournal of the American Ceramic Society
Volume82
Issue number2
Publication statusPublished - 1999 Feb 1

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Colloids
Zirconia
Electron microscopy
Salts
Elastic scattering
Light scattering
Nucleation
Agglomeration
Crystallization
Particle size
zirconium oxide

All Science Journal Classification (ASJC) codes

  • Ceramics and Composites
  • Materials Chemistry

Cite this

Lee, K., Sathyagal, A., Carr, P. W., & McCormick, A. V. (1999). Synthesis of Zirconia Colloids from Aqueous Salt Solutions. Journal of the American Ceramic Society, 82(2), 338-342.
Lee, Kangtaek ; Sathyagal, Arun ; Carr, Peter W. ; McCormick, Alon V. / Synthesis of Zirconia Colloids from Aqueous Salt Solutions. In: Journal of the American Ceramic Society. 1999 ; Vol. 82, No. 2. pp. 338-342.
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Lee, K, Sathyagal, A, Carr, PW & McCormick, AV 1999, 'Synthesis of Zirconia Colloids from Aqueous Salt Solutions', Journal of the American Ceramic Society, vol. 82, no. 2, pp. 338-342.

Synthesis of Zirconia Colloids from Aqueous Salt Solutions. / Lee, Kangtaek; Sathyagal, Arun; Carr, Peter W.; McCormick, Alon V.

In: Journal of the American Ceramic Society, Vol. 82, No. 2, 01.02.1999, p. 338-342.

Research output: Contribution to journalArticle

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